Articles | Volume 8, issue 3
https://doi.org/10.5194/gchron-8-447-2026
https://doi.org/10.5194/gchron-8-447-2026
Short communication/technical note
 | 
10 Aug 2026
Short communication/technical note |  | 10 Aug 2026

Technical note: Design, construction, automation, and first-principles calibration of a low volume He measurement line

James R. Metcalf and Rebecca M. Flowers

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Cited articles

Danišík, M., McInnes, B. I. A., Kirkland, C. L., McDonald, B. J., Evans, N. J., and Becker, T.: Seeing is believing: Visualization of He distribution in zircon and implications for thermal history reconstruction on single crystals, Science Advances, 3, e1601121, https://doi.org/10.1126/sciadv.1601121, 2017. 
Farley, K. A., Reiners, P. W., and Nenow, V.: An Apparatus for High-Precision Helium Diffusion Measurements from Minerals, Anal. Chem., 71, 2059–2061, https://doi.org/10.1021/ac9813078, 1999. 
Gautheron, C., Pinna-Jamme, R., Derycke, A., Ahadi, F., Sanchez, C., Haurine, F., Monvoisin, G., Barbosa, D., Delpech, G., Maltese, J., Sarda, P., and Tassan-Got, L.: Technical note: Analytical protocols and performance for apatite and zircon (U–Th) / He analysis on quadrupole and magnetic sector mass spectrometer systems between 2007 and 2020, Geochronology, 3, 351–370, https://doi.org/10.5194/gchron-3-351-2021, 2021. 
Henins, I.: Precision density measurement of silicon, J. Res. Nbs. A Phys. Ch., 68, 529, https://doi.org/10.6028/jres.068A.050, 1964. 
House, M. A., Farley, K. A., and Stockli, D.: Helium chronometry of apatite and titanite using Nd-YAG laser heating, Earth Pl. Sc. Lett., 183, 365–368, https://doi.org/10.1016/s0012-821x(00)00286-7, 2000. 
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Short summary
(U-Th)/He chronology requires measuring the absolute amount of radiogenic He in a sample. While high-quality commercial He lines are available, these machines are not always ideal for researchers interested in developing new or emerging techniques like laser ablation (U-Th)/He chronology. This manuscript describes the design, construction, automation, and calibration of a new He analysis line in the University of Colorado Thermochronology Research and Instrumentation Lab (CU TRaIL) facility that is optimized for measuring small amounts of He.
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