Articles | Volume 5, issue 2
https://doi.org/10.5194/gchron-5-361-2023
https://doi.org/10.5194/gchron-5-361-2023
Short communication/technical note
 | 
20 Sep 2023
Short communication/technical note |  | 20 Sep 2023

Technical note: Studying lithium metaborate fluxes and extraction protocols with a new, fully automated in situ cosmogenic 14C processing system at PRIME Lab

Nathaniel Lifton, Jim Wilson, and Allie Koester

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Revised manuscript accepted for GChron
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Cited articles

Donahue, D. J., Jull, A. J. T., and Toolin, L.: Radiocarbon measurements at the University of Arizona AMS facility, Nucl. Instrum. Meth. B, 52, 224–228, 1990. 
Fülöp, R., Naysmith, P., Cook, G., and Fabel, D.: Update on the performance of the SUERC in situ cosmogenic 14C extraction line, Radiocarbon, 52, 1288–1294, 2010. 
Fülöp, R. H., Wacker, L., and Dunai, T. J.: Progress report on a novel in situ 14C extraction scheme at the University of Cologne, Nucl. Instrum. Meth. B, 361, 20–24, https://doi.org/10.1016/j.nimb.2015.02.023, 2015. 
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Short summary
We describe a new, fully automated extraction system for in situ 14C at PRIME Lab that incorporates more reliable components and designs than our original systems. We use a LiBO2 flux to dissolve a quartz sample in oxygen after removing contaminant 14C with a lower-temperature combustion step. Experiments with new Pt/Rh sample boats demonstrated reduced procedural blanks, and analyses of well-characterized intercomparison materials tested the effects of process variables on 14C yields.